HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 5-bromo-2-methylbenzoate → HCID 51033432, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 5-bromo-2-methylbenzoate | HCID 316201 | — |
| Reactant | HCID 67043969 | HCID 67043969 | — |
| Product | HCID 51033432 | HCID 51033432 | — |
Reaction Steps
The title compound was prepared in analogy to Example 1 starting from 5-bromo-2-methyl-benzoic acid methyl ester (commercially available) and 3-[1-phenyl-eth-(E)-ylidene]-1,3-dihydro-indol-2-one. 1H NMR (400 MHz, chloroform-d) δppm 2.71 (s, 3H) 2.86 (s, 3H) 3.91 (s, 3H) 6.24 (d, J=7.83 Hz, 1H) 6.67-6.75 (m, 2H) 7.08 (t, J=7.83 Hz, 1H) 7.34-7.37 (m, 2H) 7.43-7.47 (m, 1H) 7.49-7.56 (m, 4H) 8.05 (d, J=2.27 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08778973B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-a03e829a358f4609b2687d0e949b45b3 |
| Source note | uspto-grants-2014_07 |