1-Chloro-4-iodobenzene → HCID 51033660, compound

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Reaction Steps

The title compound was prepared in analogy to Example 5 starting from 1-chloro-4-iodo-benzene (commercially available) and 3-{[(4-fluoro-phenyl)-(3-phenyl-propynoyl)-amino]-methyl}-benzoic acid methyl ester. 1H NMR (300 Hz, CDCl3): δppm 3.91 (s, 3H), 4.94 (s, 2H), 6.25 (dd, 1H), 6.54 (dd, 2H), 6.75-6.80 (m, 1H), 7.10 (d, 2H), 7.33-7.54 (m, 8H), 7.94 (d, 1H), 7.98 (s, 1H).

Provenance & Evidence