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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1623449Generated: October 31, 2026

1,3-Dichloro-5-iodobenzene → HCID 51033775, compound

https://huagongshe.com/reaction/1623449

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,3-Dichloro-5-iodobenzeneHCID 76424—
Reactant3-{[Phenyl-(3-phenyl propynoyl)-amino]-methyl}-benzoic acid methyl esterHCID 67036155—
ProductHCID 51033775HCID 51033775—

Reaction Steps

The title compound was prepared in analogy to Example 5 starting from 1,3-dichloro-5-iodobenzene (commercially available) and 3-{[phenyl-(3-phenyl propynoyl)-amino]-methyl}-benzoic acid methyl ester. 1H NMR (300 Hz, CDCl3): δppm 3.92 (s, 3H), 4.95 (s, 2H), 6.47 (d, 1H), 6.65-6.78 (m, 2H), 7.13 (t, 2H), 7.33-7.43 (m, 8H), 7.52 (d, 1H), 7.93 (d, 1H), 8.01 (s, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08778973B2
Source datasetuspto-grants-2014_07
ORD IDord-33216be31b7d427f8d86067c2a1929f3
Source noteuspto-grants-2014_07