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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1623450Generated: November 3, 2026

1,2-Dichloro-3-iodobenzene → HCID 51033776, compound

https://huagongshe.com/reaction/1623450

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,2-Dichloro-3-iodobenzeneHCID 75459—
Reactant3-{[Phenyl-(3-phenyl propynoyl)-amino]-methyl}-benzoic acid methyl esterHCID 67036155—
ProductHCID 51033776HCID 51033776—

Reaction Steps

The title compound was prepared in analogy to Example 5 starting from 1,2-dichloro-3-iodobenzene (commercially available) and 3-{[phenyl-(3-phenyl propynoyl)-amino]-methyl}-benzoic acid methyl ester. 1H NMR (CDCl3, 300 MHz) δppm 8.00 (s, 1H), 7.92 (d, 1H), 7.33-7.54 (m, 9H), 7.23 (dd, 1H), 7.10 (t, 1H), 6.74 (t, 1H), 6.66 (d, 1H), 6.55 (d, 1H), 4.95 (s, 2H), 3.90 (s, 3H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08778973B2
Source datasetuspto-grants-2014_07
ORD IDord-91c5a91db2754fa49955935e1542037b
Source noteuspto-grants-2014_07