HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-bromo-3-iodo- → HCID 51034988, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-bromo-3-iodo- | HCID 11561 | — |
| Reactant | 3-{[Phenyl-(3-phenyl propynoyl)-amino]-methyl}-benzoic acid methyl ester | HCID 67036155 | — |
| Product | HCID 51034988 | HCID 51034988 | — |
Reaction Steps
The title compound was prepared in analogy to Example 5 starting from 1-bromo-3-iodobenzene (commercially available) and 3-{[phenyl-(3-phenyl propynoyl)-amino]-methyl}-benzoic acid methyl ester. 1H NMR (CDCl3, 300 MHz) δppm 8.01 (s, 1H), 7.93 (d, 1H), 7.31-7.61 (m, 11H), 7.08 (t, 1H), 6.64-6.73 (m, 2H), 6.44 (d, 1H), 4.95 (s, 2H), 3.91 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08778973B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-3dc57ef0620c47bb9a62758cbb6acbe8 |
| Source note | uspto-grants-2014_07 |