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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1623457Generated: November 2, 2026

Benzene, 1-bromo-3-iodo- → HCID 51034988, compound

https://huagongshe.com/reaction/1623457

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzene, 1-bromo-3-iodo-HCID 11561—
Reactant3-{[Phenyl-(3-phenyl propynoyl)-amino]-methyl}-benzoic acid methyl esterHCID 67036155—
ProductHCID 51034988HCID 51034988—

Reaction Steps

The title compound was prepared in analogy to Example 5 starting from 1-bromo-3-iodobenzene (commercially available) and 3-{[phenyl-(3-phenyl propynoyl)-amino]-methyl}-benzoic acid methyl ester. 1H NMR (CDCl3, 300 MHz) δppm 8.01 (s, 1H), 7.93 (d, 1H), 7.31-7.61 (m, 11H), 7.08 (t, 1H), 6.64-6.73 (m, 2H), 6.44 (d, 1H), 4.95 (s, 2H), 3.91 (s, 3H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08778973B2
Source datasetuspto-grants-2014_07
ORD IDord-3dc57ef0620c47bb9a62758cbb6acbe8
Source noteuspto-grants-2014_07