HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-4-iodobenzene → HCID 58201655, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-4-iodobenzene | HCID 12510 | — |
| Reactant | HCID 67036281 | HCID 67036281 | — |
| Product | HCID 58201655 | HCID 58201655 | — |
Reaction Steps
The title compound was prepared in analogy to Example 5 starting from 1-chloro-4-iodo-benzene (commercially available) and 3-{[(2-chloro-4-fluoro-phenyl)-(3-phenyl-propynoyl)-amino]-methyl}-benzoic acid methyl ester. 1H NMR (300 Hz, CDCl3): δppm 3.90 (s, 3H), 5.38 (s, 2H), 6.01 (dd, 1H), 6.80 (dd, 1H), 7.27-7.40 (m, 9H), 7.45-7.50 (m, 3H), 7.92 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08778973B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-8be25276a2b5478683c4133d4bbd2ec6 |
| Source note | uspto-grants-2014_07 |