HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Iodothiophene → HCID 51033779, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Iodothiophene | HCID 66332 | — |
| Reactant | 3-{[Phenyl-(3-phenyl propynoyl)-amino]-methyl}-benzoic acid methyl ester | HCID 67036155 | — |
| Product | HCID 51033779 | HCID 51033779 | — |
Reaction Steps
The title compound was prepared in analogy to Example 5 starting from 3-iodo-thiophene (commercially available) and 3-{[phenyl-(3-phenyl propynoyl)-amino]-methyl}-benzoic acid methyl ester. 1H NMR (300 Hz, CDCl3): δppm 3.91 (s, 3H), 4.96 (s, 2H), 6.65 (d, 1H), 6.76-6.82 (m, 2H), 7.06-7.11 (m, 2H), 7.33-7.43 (m, 8H), 7.50 (d, 1H), 7.92 (d, 1H), 8.01 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08778973B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-426023d38f3e4f3485e76a9b9cd1cb81 |
| Source note | uspto-grants-2014_07 |