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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1623463Generated: October 31, 2026

3-Iodothiophene → HCID 51033779, compound

https://huagongshe.com/reaction/1623463

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-IodothiopheneHCID 66332—
Reactant3-{[Phenyl-(3-phenyl propynoyl)-amino]-methyl}-benzoic acid methyl esterHCID 67036155—
ProductHCID 51033779HCID 51033779—

Reaction Steps

The title compound was prepared in analogy to Example 5 starting from 3-iodo-thiophene (commercially available) and 3-{[phenyl-(3-phenyl propynoyl)-amino]-methyl}-benzoic acid methyl ester. 1H NMR (300 Hz, CDCl3): δppm 3.91 (s, 3H), 4.96 (s, 2H), 6.65 (d, 1H), 6.76-6.82 (m, 2H), 7.06-7.11 (m, 2H), 7.33-7.43 (m, 8H), 7.50 (d, 1H), 7.92 (d, 1H), 8.01 (s, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08778973B2
Source datasetuspto-grants-2014_07
ORD IDord-426023d38f3e4f3485e76a9b9cd1cb81
Source noteuspto-grants-2014_07