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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1623718Generated: November 3, 2026

HCID 67106787, compound → HCID 67108014, compound

https://huagongshe.com/reaction/1623718

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67106787HCID 67106787—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 67108014HCID 67108014—

Reaction Steps

To a suspension of ethyl (2Z)-3-{4-[(phenylmethyl)oxy]-3-[(3-pyridinylamino)carbonyl]phenyl}-2-propenoate (may be prepared as described in Example 68; 160 mg, 0.40 mmol) in methanol (10 ml) was added Pd/C (20 mg). The mixture was put under a hydrogen atmosphere for 5 hours. The catalyst was removed by filtration through Celite and the solvent removed in vacuo to yield the title compound as a pale yellow solid. 119 mg.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08778939B2
Source datasetuspto-grants-2014_07
ORD IDord-3092405061e048f087271a742b58ab94
Source noteuspto-grants-2014_07