1,2-Dichloroethane → HCID 68107702, compound

Participants

Reaction Steps

A solution of 5-fluoro-2-[(phenylmethyl)oxy]benzoic acid (may be prepared as described in Description 20, 180 mg, 0.73 mmol), 3-pyridinamine (68.8 mg, 0.73 mmol), HOBT (134 mg, 0.88 mmol) and EDC (168 mg, 0.88 mmol) in DMF (10 ml) was stirred at room temperature overnight. Water (30 ml) was added and the mixture was filtered. The residue was dried to yield the title compound as a white solid. 100 mg.

Provenance & Evidence