Lithium Hydroxide → HCID 69937006, compound

Participants

Reaction Steps

Lithium hydroxide (9.24 mg, 0.39 mmol) was added to a solution of ethyl 3-{4-[(phenylmethyl)oxy]-3-[(3-pyridinylamino)carbonyl]phenyl}propanoate (may be prepared as described in Example 87; 52 mg, 0.13 mmol) in tetrahydrofuran (2 ml) and water (0.5 ml) and the mixture was stirred overnight. The reaction mixture was purified by MDAP to yield the title compound as a golden solid. 62 mg.

Provenance & Evidence