HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 67060899, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | 3-(Aminomethyl)-N,N-dimethylthiolan-3-amine | HCID 2779827 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 67060899 | HCID 67060899 | — |
Reaction Steps
To a stirred solution of 3-(aminomethyl)-N,N-dimethyltetrahydrothiophen-3-amine (160 mg, 0.998 mmol) in DCM: MeOH (4:1, 10 mL) was added MCPBA (246 mg, 1.098 mmol) at 0° C. The reaction was slowly warmed to room temperature and stirred overnight. The crude was purified by cation exchange resin to give the title compound without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08778950B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-57b5fb611b004847b18e18eda2bb163f |
| Source note | uspto-grants-2014_07 |