HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofurfuryl alcohol → HCID 70655756, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofurfuryl alcohol | HCID 7360 | — |
| Reactant | Silane, (chloromethyl)diethoxymethyl- | HCID 16650 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Catalyst | Potassium Iodide | HCID 4875 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 70655756 | HCID 70655756 | — |
Reaction Steps
Under conditions similar to Example 3, the reaction product of sodium metal and tetrahydrofurfuryl alcohol was reacted with chloromethylmethyldiethoxysilane in the presence of potassium iodide catalyst in toluene. The reaction proceeded to the desired product only to the extent of 20% with the formation of significant amounts of byproducts.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08779080B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-a65827bac08f4779b3dc75503d42a238 |
| Source note | uspto-grants-2014_07 |