HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dibromoethane → HCID 178505629, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dibromoethane | HCID 7839 | — |
| Reactant | Zinc | HCID 23994 | — |
| Reactant | alpha-Bromo-o-fluorotoluene | HCID 67968 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178505629 | HCID 178505629 | — |
Reaction Steps
2-Fluoro-benzyl bromide (1 g, 5.29 mmol), zinc (0.380 g, 5.82 mmol) and 1,2-dibromoethane (0.050 mL, 0.58 mmol) were mixed in THF (10 ML) and heated to reflux overnight. After cooling a solution of the title compound was obtained that was used directly and immediately in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08778983B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-158b6badf40d48f3b6629f02307e00c8 |
| Source note | uspto-grants-2014_07 |