2-(Bromomethyl)pyridine hydrobromide → HCID 57330882, compound

Participants

Reaction Steps

Prepared in a similar manner to example 1 using 5-(2,5-dimethylfuran-3-yl)-2H-1,2,4-triazole-3(4H)-thione (example 7a) and 2-(bromomethyl)pyridine hydrobromide. Yield 70%. 1H NMR (500 MHz, CDCl3): δ 2.27 (s, 3H), 2.59 (s, 3H), 4.32 (s, 2H), 6.35 (s, 1H), 7.28-7.29 (d, 1H), 7.35-7.36 (d, 1H), 7.75 (t, 1H) 8.62 (s, 1H). MS (M+H, 287).

Provenance & Evidence