HRID1625667

反应详情

EQUATION

反应方程式

HRID 1625667 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

[2′-[(tert-Butoxycarbonyl-ethyl-amino)-methyl]-4′-(6-ethoxy-pyridin-3-yl)-6-methoxy-biphenyl-3-yl]-acetic acid ethyl ester (0.404 g, 0.736 mmol) in dichloromethane (3 mL) was treated with 4N hydrochloric acid in 1,4-dioxane (2.5 mL, 10 mmol) at room temperature, until complete conversion was seen by analytical LCMS. The mixture was concentrated to give the title compound.

WORKUP

后处理

  1. concentrationThe mixture was concentrated