4-Ethylbenzaldehyde → HCID 63796624, compound

HRID 1625841Notes

Reaction equation

HRID 1625841 reaction equation
Br[C:2]1[S:3][CH:4]=[CH:5][C:6]=1[Br:7].[CH2:8]([C:10]1[CH:17]=[CH:16][C:13]([CH:14]=[O:15])=[CH:12][CH:11]=1)[CH3:9]>>[Br:7][C:6]1[CH:5]=[CH:4][S:3][C:2]=1[CH:14]([C:13]1[CH:16]=[CH:17][C:10]([CH2:8][CH3:9])=[CH:11][CH:12]=1)[OH:15]

Participants

3

Reactant 2

HCID 208614-EthylbenzaldehydeHCID 765902,3-Dibromothiophene

Product 1

HCID 63796624HCID 63796624, compound

Procedure

2,3-Dibromothiophene and 4-ethylbenzaldehyde were treated in a manner similar to Reference Example 1-(1) to give 3-bromo-2-thienyl-4-ethylphenylmethanol as yellow oil. APCI-Mass m/Z 279/281 (M+H−H2O).

Sources & evidence

ORD record
ord-0c6e3e8d2fd046c683adc2f59afc55cf
Source dataset
uspto-grants-2014_07
Patent number
US08785403B2

Reaction notes

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