HRID1626079

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID11355477

tert-Butylsulfinamide, (S)-(-)-

C4H11NOS

HCID54857833

未命名化合物

PRODUCTS

生成物

$结构：CC(C)(C)[S@](=O)/N=C(\c1cc(Br)ccc1F)C(F)F$

HCID89183621

未命名化合物

收率 78%

PROCEDURE

实验过程

Starting from 1-(5-bromo-2-fluorophenyl)-2,2-difluoroethanone and (S)-(−)-2-methyl-2-propanesulfinamide, the (S,E)-N-(1-(5-bromo-2-fluorophenyl)-2,2-difluoroethylidene)-2-methylpropane-2-sulfinamide (14.49 g, 78.0% yield) was obtained as a yellow oil. MS (ISP): m/z=355.9 [M+H]+ and 357.9 [M+2+H]+.