HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 178452218, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | tert-Butyl piperazine-1-carboxylate | HCID 143452 | — |
| Reactant | HCID 86667008 | HCID 86667008 | — |
| Product | HCID 178452218 | HCID 178452218 | — |
Reaction Steps
A solution of 1-trifluoromethylphenothiazin-5-ium tetraiodide hydrate (150 mg, 0.19 mmol) in methanol (10 mL) and 1-Boc-piperazine (93 mg, 0.5 mmol) was stirred for 4 h at room temperature. The resulting mixture was concentrated to dryness and purified by flash chromatography using the methanol-chloroform gradient to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785434B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-48d7c06f9b5747b394d1a098c2c6051d |
| Source note | uspto-grants-2014_07 |