HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 178448937, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 178448939 | HCID 178448939 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178448937 | HCID 178448937 | — |
Reaction Steps
A solution of 3-(4-Boc-piperazin-1-yl)-7-(methyl(n-butyl)amino)-1,9-dimethylphenothiazin-5-ium iodide (25 mg) in dichloromethane (5 mL) and trifluoroacetic acid (2 mL) was stirred for 4 h at room temperature. The resulting mixture was concentrated to dryness, rinsed out by toluene (3×10 mL) and dried under vacuum to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785434B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-1a98abd29ac642f9b9afd949d66e6f4b |
| Source note | uspto-grants-2014_07 |