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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1626263Generated: October 30, 2026

Trifluoroacetic acid → HCID 178448937, compound

https://huagongshe.com/reaction/1626263

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 178448939HCID 178448939—
SolventDichloromethaneHCID 6344—
ProductHCID 178448937HCID 178448937—

Reaction Steps

A solution of 3-(4-Boc-piperazin-1-yl)-7-(methyl(n-butyl)amino)-1,9-dimethylphenothiazin-5-ium iodide (25 mg) in dichloromethane (5 mL) and trifluoroacetic acid (2 mL) was stirred for 4 h at room temperature. The resulting mixture was concentrated to dryness, rinsed out by toluene (3×10 mL) and dried under vacuum to provide the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08785434B2
Source datasetuspto-grants-2014_07
ORD IDord-1a98abd29ac642f9b9afd949d66e6f4b
Source noteuspto-grants-2014_07