HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazine → HCID 178436997, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | 1-Ethyl-9-methylphenothiazin-5-ium tetraiodide hydrate | HCID 86667030 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178436997 | HCID 178436997 | — |
Reaction Steps
A solution of 1-ethyl-9-methylphenothiazin-5-ium tetraiodide hydrate (50 mg, 0.07 mmol) in methanol (10 mL) and 1-methylpiperazine (30 mg, 0.3 mmol) was stirred for 2 h at room temperature. The resulting mixture was concentrated to dryness and purified by flash chromatography using the methanol-chloroform gradient to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785434B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-c08096aee9514845a0d8d3545066df5a |
| Source note | uspto-grants-2014_07 |