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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1626267Generated: November 2, 2026

Methanol → HCID 178436810, compound

https://huagongshe.com/reaction/1626267

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
Reactant1-MethylpiperazineHCID 53167—
ReactantHCID 178435889HCID 178435889—
ProductHCID 178436810HCID 178436810—

Reaction Steps

A solution of 3-(bis(2-methoxyethyl)amino)-9-ethyl-1-methylphenothiazin-5-ium triiodide (150 mg, 0.2 mmol) in methanol (10 mL) and 1-methylpiperazine (30 mg, 0.3 mmol) was stirred for 2 h at room temperature. The resulting mixture was concentrated to dryness and purified by flash chromatography using the methanol-chloroform gradient to provide the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08785434B2
Source datasetuspto-grants-2014_07
ORD IDord-c2f591c3366c44c9afe81847fe60da07
Source noteuspto-grants-2014_07