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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1626271Generated: October 30, 2026

HCID 178436738, compound → HCID 178436734, compound

https://huagongshe.com/reaction/1626271

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178436738HCID 178436738—
SolventDichloromethaneHCID 6344—
SolventTrifluoroacetic acidHCID 6422—
ProductHCID 178436734HCID 178436734—

Reaction Steps

a solution of 3,7-bis(4-Boc-1,4-diazepan-1-yl)-1-ethyl-9-methyl-phenothiazin-5-ium iodide (75 mg, 0.01 mmol) in dichloromethane (10 mL) and trifluoroacetic acid (1.0 mL) was stirred for 3 h at 50° C. The resulting mixture was washed by toluene (2×5 mL), pentane (2×5 mL) and concentrated to dryness.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08785434B2
Source datasetuspto-grants-2014_07
ORD IDord-bc5c998a4f8f4fc884d3525149b7b85e
Source noteuspto-grants-2014_07