HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178436738, compound → HCID 178436734, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178436738 | HCID 178436738 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 178436734 | HCID 178436734 | — |
Reaction Steps
a solution of 3,7-bis(4-Boc-1,4-diazepan-1-yl)-1-ethyl-9-methyl-phenothiazin-5-ium iodide (75 mg, 0.01 mmol) in dichloromethane (10 mL) and trifluoroacetic acid (1.0 mL) was stirred for 3 h at 50° C. The resulting mixture was washed by toluene (2×5 mL), pentane (2×5 mL) and concentrated to dryness.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785434B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-bc5c998a4f8f4fc884d3525149b7b85e |
| Source note | uspto-grants-2014_07 |