HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66680278, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 86661493 | HCID 86661493 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 66680278 | HCID 66680278 | 82.1% |
Reaction Steps
10 mL of ethanol and 4.0 mL of 1N aqueous sodium hydroxide solution were added to 615 mg (2.50 mmol) of ethyl [3-(furan-2-yl)phenoxy]acetate, and the mixture was stirred at room temperature for 4 hours. 1N hydrochloric acid was added to acidify the reaction mixture, and water was added thereto. The precipitated solids were collected by filtration, washed with water, and air-dried, thereby giving 448 mg of [3-(furan-2-yl)phenoxy]acetic acid (yield: 82%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785473B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-59ffac7b100e4c908a6f92f068c544a9 |
| Source note | uspto-grants-2014_07 |