化工社化工社 化学情報印刷レポート · 研究参考用
(4-Bromophenyl)boronic acid → Ethyl 6-(4-bromophenyl)nicotinate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (4-Bromophenyl)boronic acid | HCID 79599 | — |
| 反応物 | Ethyl 6-bromonicotinate | HCID 14784668 | — |
| 生成物 | Ethyl 6-(4-bromophenyl)nicotinate | HCID 68193233 | 98% |
反応手順
In accordance with Example 11-(1), but using ethyl 6-bromonicotinate instead of 4-bromobenzylbromide, and 4-bromophenylboronic acid instead of [3-(hydroxymethyl)phenyl]boronic acid, the title compound (yield 98%) was afforded as a white solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08785462B2 |
| 出典データセット | uspto-grants-2014_07 |
| ORD ID | ord-ed36ab0287a34f0ca47e1ec93bfc6434 |
| 出典メモ | uspto-grants-2014_07 |