HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2-iodotoluene → HCID 68193177, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2-iodotoluene | HCID 2724601 | — |
| Reactant | 4-(Hydroxymethyl)benzeneboronic acid | HCID 2734706 | — |
| Product | HCID 68193177 | HCID 68193177 | 7.1% |
Reaction Steps
In accordance with Example 4-(2), but using [4-(hydroxymethyl)phenyl]boronic acid instead of (4-bromophenyl)boronic acid, and 4-bromo-1-iodo-2-methylbenzene instead of tert-butyl[2-(4-iodophenyl)ethoxy]dimethylsilane, the title compound (yield 7.1%) was afforded as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785462B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-2dcc654203b646679d9192c90dbb475b |
| Source note | uspto-grants-2014_07 |