2-(3-Nitro-4-hydroxyphenyl)propionic acid → HCID 12202637, compound

Participants

Reaction Steps

A mixture of (1) (810 mg, 1 mmol) in THF (20 ml) and EtOH (20 ml) is slowly added to 10% Pd/C (90 mg) at room temperature. The reaction mixture is hydrogenated for 3 h with H2 balloon at 45 psi. The mixture is filtered through celite pad and washed with EtOH. The filtrate is concentrated in vacuo.

Provenance & Evidence