反应详情

A mixture of (1) (810 mg, 1 mmol) in THF (20 ml) and EtOH (20 ml) is slowly added to 10% Pd/C (90 mg) at room temperature. The reaction mixture is hydrogenated for 3 h with H2 balloon at 45 psi. The mixture is filtered through celite pad and washed with EtOH. The filtrate is concentrated in vacuo.

1. filtrationThe mixture is filtered through celite pad
2. washwashed with EtOH
3. concentrationThe filtrate is concentrated in vacuo