反应详情

A mixture of D2 (16 g, 90.39 mmol) in NH4OH (100 ml, 30% in water) was heated at reflux for 3 h. After cooling in an ice bath a yellow solid precipitated. The solid was filtered off, washed with cold isopropanol and dried in vacuo to yield compound D3 (10 g, 76%) as a white solid.

1. temperaturewas heated
2. temperatureat reflux for 3 h
3. temperatureAfter cooling in an ice bath a yellow solid
4. customprecipitated
5. filtrationThe solid was filtered off
6. washwashed with cold isopropanol
7. customdried in vacuo