TIBA cyclohexane → 2,3,5-Triiodobenzoic acid

Participants

Reaction Steps

18.2 mL of TIBA/cyclohexane solution (99 g/L) were mixed with 3.8 mL of MAO/toluene solution to obtain a MAO/TIBA molar ratio of 2:1. The solution was stirred for 1 h at room temperature and transferred into a 50 mL Schlenk flask containing A-1 (37.3 mg, 45.4 μmol). The final solution was diluted with 35.9 mL of cyclohexane. Final mixture concentration=50 gTOT/L and 0.645 gmetallocene/L; color=orange solution.

Provenance & Evidence