Hydrochloric Acid → HCID 178489935, compound

Participants

Reaction Steps

A solution of 2-(2-(3,4-dimethoxyphenyl)acetyl)-N-(4-fluorophenyl)hydrazine-carbothioamide (2.03 g) in 2N NaOH (200 mL) was heated at reflux 3 h. The reaction was cooled and acidified to pH 5 with 2N HCl. White solids precipitated, were collected by filtration and washed with water. The solids were dried under vacuum to yield the title compound (1.56 g, 81%).

Provenance & Evidence