HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl acrylate → HCID 24859311, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl acrylate | HCID 15458 | — |
| Reactant | HCID 10869380 | HCID 10869380 | — |
| Product | HCID 24859311 | HCID 24859311 | 95% |
Reaction Steps
The representative procedure was followed using tert-butyl(dec-9-enyloxy)dimethylsilane (135 mg, 0.50 mmol), tert-butyl acrylate (128 mg, 1.00 mmol) and Grubbs-2 catalyst (8.5 mg, 0.01 mmol). Column chromatography on silica gel (eluting with 2% EtOAc/hexanes) afforded the product as a colorless oil (176 mg, 95%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785665B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-20931112c79c426393e4d2936545be6f |
| Source note | uspto-grants-2014_07 |