HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl acrylate → HCID 58288927, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl acrylate | HCID 15458 | — |
| Reactant | HCID 11482047 | HCID 11482047 | — |
| Product | HCID 58288927 | HCID 58288927 | 91% |
Reaction Steps
The representative procedure was followed using tert-butyl(2-allylphenoxy)dimethylsilane (124 mg, 0.50 mmol), tert-butyl acrylate (128 mg, 1.00 mmol) and Grubbs-2 catalyst (8.5 mg, 0.01 mmol). Column chromatography on silica gel (eluting with 3% EtOAc/hexanes) afforded the product as a colorless oil (158 mg, 91%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785665B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-bdfea253a2204b57808af527dfdca1a6 |
| Source note | uspto-grants-2014_07 |