HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl vinyl ketone → HCID 53342911, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl vinyl ketone | HCID 6570 | — |
| Reactant | HCID 11482047 | HCID 11482047 | — |
| Product | HCID 53342911 | HCID 53342911 | 74% |
Reaction Steps
The representative procedure was followed using tert-butyl(2-allylphenoxy)dimethylsilane (124 mg, 0.50 mmol), methyl vinyl ketone (106 mg, 1.50 mmol) and Grubbs-2 catalyst (8.5 mg, 0.01 mmol). Column chromatography on silica gel (eluting with 3% EtOAc/hexanes) afforded the product as a colorless oil (107 mg, 74%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785665B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-74608cf3920340f1a17167220eb34ebb |
| Source note | uspto-grants-2014_07 |