HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl acrylate → HCID 11218554, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl acrylate | HCID 15458 | — |
| Reactant | 4-Iodoanisole | HCID 69676 | — |
| Product | HCID 11218554 | HCID 11218554 | 97% |
Reaction Steps
Following the general procedure using 4-methoxyiodobenzene (117 mg, 0.50 mmol) and tert-butyl acrylate (145 μL, 1.00 mmol), the reaction was stirred for 4 h at rt. Column chromatography on silica gel (eluting with 3% EtOAc/hexanes) afforded the product as a colorless oil (113 mg, 97%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785665B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-dc4a94e632f24f358d26512cba3e9c91 |
| Source note | uspto-grants-2014_07 |