HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dimethylstyrene → HCID 58288925, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dimethylstyrene | HCID 16694 | — |
| Reactant | 1-iodo-2-methoxynaphthalene | HCID 269493 | — |
| Product | HCID 58288925 | HCID 58288925 | 95% |
Reaction Steps
Following the general procedure using 1-iodo-2-methoxynaphthalene (142 mg, 0.50 mmol) and 2,4-dimethylstyrene (132 μL, 1.0 mmol), the reaction was stirred for 12 h at rt. Column chromatography on silica gel (eluting with 5% EtOAc/hexanes) afforded the product as a tan semi-solid (137 mg, 95%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785665B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-6fcf37cf2e5a41db9fc9256bfeddb8db |
| Source note | uspto-grants-2014_07 |