HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminopyridine → HCID 67215728, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminopyridine | HCID 10009 | — |
| Reactant | 3-Bromotoluene | HCID 11560 | — |
| Product | HCID 67215728 | HCID 67215728 | 98% |
Reaction Steps
Following the general procedure using 3-bromotoluene (121 μL, 1.00 mmol) and 3-aminopyridine (113 mg, 1.20 mmol), the reaction was stirred for 20 h at rt. Column chromatography on silica gel (eluting with 40% EtOAc/hexanes) afforded the product as an off-white solid (180 mg, 98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785665B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-44cdc59b1ae247c1896f6b9cc883cb45 |
| Source note | uspto-grants-2014_07 |