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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1628250Generated: November 3, 2026

Potassium Carbonate → HCID 67496215, compound

https://huagongshe.com/reaction/1628250

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 67497428HCID 67497428—
SolventMethanolHCID 887—
ProductHCID 67496215HCID 67496215—

Reaction Steps

To (R)-1-(1-ethyl-3-(pyridin-4-yl)-1H-pyrazol-5-ylamino)-1-oxo-3-phenylpropan-2-yl acetate (438 mg, 1157 μmol) was added K2CO3 (320 mg, 2315 μmol), followed by MeOH. After 1 hr, the reaction was completed by LC/MS. The reaction was concentrated and worked up with brine and 30% isopropanol in CHCl3. The crude material was purified by trituration with dichloromethane followed by filtration.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08785468B2
Source datasetuspto-grants-2014_07
ORD IDord-f9645a33045643949bf2d5422fbf6032
Source noteuspto-grants-2014_07