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HRID1628279

反应详情

EQUATION

反应方程式

HRID 1628279 的结构方程式

REACTANTS

反应物

2
结构：CC(C)n1nc(-c2ccncc2)cc1N
HCID67496076

未命名化合物

结构：CNc1cc(-c2cc(NC(=O)[C@@H](N)Cc3ccc(F)cc3)[nH]n2)ccn1
HCID178482068

未命名化合物

PRODUCTS

生成物

1
结构：CNc1cc(-c2cc(NC(=O)[C@@H](N)Cc3ccc(F)cc3)n(C(C)C)n2)ccn1
HCID67496294

未命名化合物

收率 75%

PROCEDURE

实验过程

This title compound was prepared starting from 29.A according the procedure described above for conversion of 18.0 to 18.E. The crude product was purified by flash chromatography on silica gel using 0-15% MeOH/CH2Cl2 for elution to provide 43.1 (510 mg, 75%). MS ESI (positive.) m/e: 397.1 (M+H).

WORKUP

后处理

  1. customThis title compound was prepared
  2. customThe crude product was purified by flash chromatography on silica gel using 0-15% MeOH/CH2Cl2 for elution