HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67496336, compound → HCID 67496300, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67496336 | HCID 67496336 | — |
| Reactant | HCID 67497718 | HCID 67497718 | — |
| Reactant | HCID 67498223 | HCID 67498223 | — |
| Product | HCID 67496300 | HCID 67496300 | 93.3% |
Reaction Steps
This title intermediate was prepared starting from 76.A (694 mg, 2.30 mmol) according the procedure described above for conversion of 65.D to 65.E. The crude product was purified by flash chromatography on silica gel using 0-10% MeOH/CH2Cl2 for elution to provide 76.B as colorless syrup (582 mg, 93%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785468B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-ee73288752a646b995ebd14a0825f79c |
| Source note | uspto-grants-2014_07 |