反应详情

To a flask with 78.G (280 mg, 0.81 mmol) was added 112 mg 10% Pd/C. The reaction was purged with hydrogen and stirred under hydrogen for 4 hrs. After filtering through a pad of celite, silica gel purification afforded 78.H 134 mg (52%).

1. customThe reaction was purged with hydrogen
2. filtrationAfter filtering through a pad of celite, silica gel purification