HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 16752340, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | 3,5-Dibromobenzaldehyde | HCID 622077 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 16752340 | HCID 16752340 | — |
Reaction Steps
21.38 g (0.081 mol) of 3,5-dibromobenzaldehyde, 16.82 g (0.162 mol) of phenylboronic acid and 1.04 g (0.90 mmol) of tetrakispalladium are initially introduced. 500 ml of 1 M sodium carbonate solution and 300 ml of THF are added, and the reaction is brought to reaction under reflux for 24 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08786181B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-46a56b646544431db5632c79a141259c |
| Source note | uspto-grants-2014_07 |