HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → 2,4-Bisbiphenyl-4-yl-6-(4'-vinylbiphenyl-4-yl)-1,3,5-triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 4-Vinylphenylboronic acid | HCID 2734393 | — |
| Reactant | 2,4-Bisbiphenyl-4-yl-6-(4-bromophenyl)-1,3,5-triazine | HCID 67335276 | — |
| Catalyst | HCID 178418397 | HCID 178418397 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2,4-Bisbiphenyl-4-yl-6-(4'-vinylbiphenyl-4-yl)-1,3,5-triazine | HCID 59439788 | — |
Reaction Steps
1.0 g (0.00185 mol) of 2,4-bisbiphenyl-4-yl-6-(4-bromophenyl)-1,3,5-triazine, 0.4106 g of 4-vinylphenylboronic acid and 0.02368 g of Pd(PPh3)4 are brought to reaction under reflux for 48 h with addition of 15 ml of 1M sodium carbonate solution and 30 ml of THF.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08786181B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-1e93f0e2168f4cb383a89eceeb4f025d |
| Source note | uspto-grants-2014_07 |