HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl acrylate → HCID 57517341, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl acrylate | HCID 15458 | — |
| Reactant | (S)-1-(3-bromophenyl)ethanamine | HCID 9952938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 57517341 | HCID 57517341 | — |
Reaction Steps
A solution of (S)-1-(3-bromo-phenyl)-ethylamine (0.3 g, 1.5 mmol) and acrylic acid tert-butyl ester (0.19 g, 1.50 mmol) in ethanol (1.3 mL) was stirred at 55° C. for 2.5 hours. The solvent was concentrated and the crude residue was purified by chromatography on silica gel (heptane/EtOAc).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08791100B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-06a8046b84264402913513ce68c0a9b8 |
| Source note | uspto-grants-2014_07 |