Hydrochloric Acid → HCID 89654098, compound

HRID 1629961Notes

Reaction equation

HRID 1629961 reaction equation
[CH3:1][C:2]1([CH3:8])[NH:6][NH:5][C:4](=[O:7])[CH2:3]1.[ClH:9]>CCOCC>[ClH:9].[CH3:1][C:2]1([CH3:8])[NH:6][NH:5][C:4](=[O:7])[CH2:3]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 111160265,5-dimethylpyrazolidin-3-one

Product 1

HCID 89654098HCID 89654098, compoundYield 100%

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

A scintillation vial equipped with a stir bar was charged with 5,5-dimethyl-pyrazolidin-3-one (228 mg, 2.0 mmol) and 2.0 M HCl in Et2O (2 mL) was added. A white PPT formed. This was filtered and washed with further Et2O (20 mL). Amount obtained: 300 mg, 2.0 mmol, 100% yield. Step 3

Workup

  1. customA scintillation vial equipped with a stir bar
  2. additionwas added
  3. customA white PPT formed
  4. filtrationThis was filtered
  5. washwashed with further Et2O (20 mL)
  6. customAmount obtained

Sources & evidence

ORD record
ord-5efcf70693b647b08269cd1e91dbf3b8
Source dataset
uspto-grants-2014_07
Patent number
US08791114B2

Reaction notes

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