HRID1630407

反应详情

EQUATION

反应方程式

HRID 1630407 的结构方程式

PROCEDURE

实验过程

818 mg of (triphenylphosphoranylidene)acetaldehyde and 500 mg of 5-bromopyridinecarbaldehyde are stirred at RT overnight. The volatile fractions are removed under reduced pressure, and the residue is purified by column chromatography (silica gel, MeOH:DCM=99:1).

WORKUP

后处理

  1. customThe volatile fractions are removed under reduced pressure
  2. customthe residue is purified by column chromatography (silica gel, MeOH:DCM=99:1)