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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1630432Generated: November 1, 2026

Cyclohexanone Oxime → HCID 57954502, compound

https://huagongshe.com/reaction/1630432

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCyclohexanone OximeHCID 7517—
ReactantChlorodifluoroacetic acidHCID 66154—
ReactantHCID 178418268HCID 178418268—
ProductHCID 57954502HCID 57954502—

Reaction Steps

1-Nitrosocyclohexyl 2-chloro-2,2-difluoroacetate was prepared from cyclohexanone oxime, lead tetraacetate and 2-chloro-2,2-difluoroacetic acid using conditions of General Method 3. 1H NMR (250 MHz, chloroform-d) δ 2.13-2.42 (3H, m), 1.79-1.99 (4H, m), 1.51-1.74 (3H, m).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08791134B2
Source datasetuspto-grants-2014_07
ORD IDord-2cbb99b5679d4b55be3e1c6e63b07f2f
Source noteuspto-grants-2014_07