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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1630434Generated: November 2, 2026

Trifluoroacetic acid → HCID 57954485, compound

https://huagongshe.com/reaction/1630434

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantN-(oxan-4-ylidene)hydroxylamineHCID 12298558—
ReactantHCID 178418268HCID 178418268—
ProductHCID 57954485HCID 57954485—

Reaction Steps

4-Nitrosotetrahydro-2H-pyran-4-yl 2,2,2-trifluoroacetate was prepared from tetrahydro-pyran-4-one oxime, lead tetraacetate and trifluoroacetic acid using conditions of General Method 3. 1H NMR (250 MHz, chloroform-d) δ 4.18 (2 H, m), 3.75 (2 H, m), 2.53 (2 H, m), 1.92 (2 H, m).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08791134B2
Source datasetuspto-grants-2014_07
ORD IDord-e40b50d7a02f4cd39008aedd8b2172d1
Source noteuspto-grants-2014_07