HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4,5-Trimethoxyaniline → HCID 59343421, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4,5-Trimethoxyaniline | HCID 32285 | — |
| Reactant | HCID 59343426 | HCID 59343426 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 59343421 | HCID 59343421 | 4% |
Reaction Steps
Using Method EE with 2-chloro-6-(indanone-7-oxy)-pyrazine (200 mg, 0.77 mmol) and 169 mg (0.92 mmol) 3,4,5-trimethoxyaniline (169 mg, 0.92 mmol), and purification by column chromatography (AcOEt), the title compound was obtained (11 mg). Yield: 4%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07737152B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-44b38a5132d74c94b773f90e0abb3709 |
| Source note | uspto-grants-2010_06 |