HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Sulfide → HCID 178494291, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Sulfide | HCID 14804 | — |
| Reactant | HCID 136337800 | HCID 136337800 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178494291 | HCID 178494291 | — |
Reaction Steps
1.3 g (4.550 mmol) of 2-chloro-4-(4-hydroxyphenyl)-6-methoxypyridine-3,5-dicarbonitrile are initially charged in 10 ml of DMF, 426 mg (5.460 mmol) of sodium sulphide are added and the mixture is stirred at room temperature overnight. The reaction mixture is reacted further without any further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08791146B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-aeeee55435c1442ab4cc263de3de1681 |
| Source note | uspto-grants-2014_07 |