HRID1631024

反应详情

EQUATION

反应方程式

HRID 1631024 的结构方程式

PROCEDURE

实验过程

The title compound was prepared following procedure described in Method B starting from Intermediate A1 and 6-chloro-N′-hydroxypyridine-3-carboximidamide (J. Med. Chem., 2005, 5215-5223). After purification by flash chromatography (silica, EtOAc/cHex), the title compound was obtained as a colorless oil (661 mg, 70%). HPLC (Method A), Rt: 5.8 min (purity: 99%). UPLC/MS, M+(ESI): 392.2.

WORKUP

后处理

  1. customThe title compound was prepared following procedure
  2. customAfter purification by flash chromatography (silica, EtOAc/cHex)